I have not tried ANY D3prefs.ini editing and everything works fine here on Nvidia hardware.
Have you set your .ini to "read only" or something that would not permit the game to edit it?
Using the in-game Video option select is all I need to do, I just tried it, switched from Fullscreen Windowed to 1920x1200 (Widescreen) and back without any issues.
Not sure what's occuring on your end.
What is your desktop resolution set to? What video card are you using?
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